Insertion Reactions of Allenes Giving Vinyl Complexes

Authors: 
Peng Xue, Jun Zhu, Herman S. Y. Hung, Ian D. Williams, Zhenyang Lin*, Guochen Jia*
Journal: 
Organometallics
Year: 
2005
Volume: 
24
FirstPage-LastPage: 
4896–4898
TOC: 
Abstract: 

Treatment of OsHCl(PPh3)(3) with allenes CH2=C=CHR at room temperature in benzene produced the vinyl complexes OsCl(C(CH3)=CHR)(CH2=C=CHR)-(PPh3)(2), instead of eta(3)-allyl complexes as normally observed. DFT calculations show that the formation of the vinyl complex is favored kinetically.

Doi: 
10.1021/om0506825